ANALYTICAL CHEMISTRY: FUNDAMENTALS

Degree course: 
Corso di First cycle degree in CHEMICAL AND INDUSTRIAL CHEMISTRY
Academic year when starting the degree: 
2020/2021
Year: 
2
Academic year in which the course will be held: 
2021/2022
Course type: 
Basic compulsory subjects
Credits: 
7
Period: 
First Semester
Standard lectures hours: 
56
Detail of lecture’s hours: 
Lesson (56 hours)
Requirements: 

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Assessment: 
Voto Finale

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Introduction: analytical chemistry and its role in research and society (2 h).
Analytical protocol: definition of the problem, choice of the analytical method, sampling, sample treatment, determination, evaluation of the results (4 h).
Equilibria in solution: electrolytes and their effects onto chemical equilibrium; ionic strength and activity; systematic approach to complex equilibria (6 h).
Gravimetric methods (2 h).
Electrochemical methods: potentiometry, conductimetry and amperometry (4 h).
Volumetric analysis: background, theory of neutralization, complexometric, redox and precipitation titrations; application of volumetric titrations (12 h).
Instrumental analysis: features of instrumental methods, block diagrams, analytical signal and calibration (4 h).
UV-visible and infrared (IR) absorption spectroscopy: theoretical aspects, instrumental apparatus and applications (8 h).
Chromatographic methods: theoretical aspects, stationary phases, detectors and applications (6 h).
Quality in analytical chemistry: quality control, quality assurance, validation, traceability, standard materials and standard analytical methods (4 h).

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The following textbook is recommended for the course:
Daniel C. Harris, Chimica Analitica Quantitativa, Zanichelli 2017
The following textbook may be also useful:
James F. Holler, Stanley R. Crouch, Fondamenti di Chimica Analitica, Edises 2015

The module features 56 hours of lecture (7 CFU). Multiple choice tests (individual activity) and real world analytical issues (group activities) will be proposed throughout the module (around 6 h). The latter aims at stimulating the ability to apply the acquired knowledge and developing the expected skills. Numerical problems will also be presented and discussed for each topic to consolidate and learn to apply the acquired knowledge and for self-evaluation purposes.

Contact the professor by e-mail at damiano.monticelli@uninsubria.it

Professors

Parent course