ORGANIC CHEMISTRY 2: LABORATORY

Degree course: 
Corso di First cycle degree in CHEMICAL AND INDUSTRIAL CHEMISTRY
Academic year when starting the degree: 
2018/2019
Year: 
2
Academic year in which the course will be held: 
2019/2020
Partizione: 
Cognomi A-L
Course type: 
Compulsory subjects, characteristic of the class
Credits: 
6
Period: 
Second semester
Standard lectures hours: 
72
Requirements: 

Knowledge of contents of General Chemistry course and of Organic Chemistry 1 course.

The students will be evaluated by their interest and diligence shown in their learning process as well as by the scientific reports of the practical experiences carried out in the laboratory. Furthermore, a final unknown practical experience will assess the acquired abilities to plan, perform, and accomplish laboratory operations in an independent and safe manner.
The topics covered in the theoretical course will be verified in the written examination of the Organic Chemistry 2 course (Module A).

Assessment: 
Voto Finale

Theoretical course: the course provides the knowledge for either recognizing the chemical hazard or working in safe conditions in an organic chemistry laboratory. It gives the theoretical knowledge of the main procedures of synthesis, purification and isolation of an organic compound. Basic introduction of the main characterization methods for organic compounds is also given.
Practical course: students will carry out simply operations of synthesis, purification and isolation of organic compounds; they will acquire the ability to recognize and to solve practical problems that may come up during a synthetic reaction or a work up. they are driven toward the acquisition of a clear scientific language through the production of scientific reports.

Theoretical course: Hazards and safety in an organic chemistry laboratory. Theoretical and practical approaches to an organic reaction. Introduction to purification techniques: crystallization, solvent extraction, simple and fractional distillation, thin layer and column chromatography. Determination of the minimum formula and of unsaturation number. Spectroscopy fundamentals (IR, NMR) for the characterization of organic functional groups.

Practical course: Synthetic reactions, fundamental operations of isolation, purification and characterization through physical properties and spectroscopic techniques of an organic compound will be performed by each student.

Theoretical course: Hazards and safety in an organic chemistry laboratory. Theoretical and practical approaches to an organic reaction. Introduction to purification techniques: crystallization, solvent extraction, simple and fractional distillation, thin layer and column chromatography. Determination of the minimum formula and of unsaturation number. Spectroscopy fundamentals (IR, NMR) for the characterization of organic functional groups.
Practical course: Synthetic reactions, fundamental operations of isolation and purification and characterization through physical properties and spectroscopic techniques of an organic compound will be performed by each student.

• D.L. Pavia – G.M. Lampman – G.S. Kriz, Il laboratorio di Chimica Organica, ed. Sorbona.
• Vogel, “Chimica Organica Pratica”, Ed. Ambrosiana.
• Antonio Randazzo, “Guida Pratica alla Interpretazione degli Spettri NMR”, Ed. Loghia.

The course will be held through 24 hours of theoretical lessons and 48 hours of laboratory experiments.

For an appointament, please contact me by email.